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更新時間：2021-01-12
ACQUITY UPLC方法驗證系統(tǒng)包提供三批色譜填料（來自不同批次的顆?；w）以判斷一個分析方法的耐受性，可靠性和一致性。
UPLC方法驗證包— 確保方法耐用性
為了確保分析方法持續(xù)可靠且具有重現性，采用多批色譜填料進行檢測和驗證變得尤為重要。作為硅膠雜化顆粒的主要生產商，沃特世公司為不同批次之間的重現性設立了行業(yè)的基準?；谛抛u*的顆粒和色譜柱生產的過程控制，使批與批和柱與柱之間的變異性小化，從而為分析方法長期的可靠性提供信心。
ACQUITY UPLC方法驗證包提供三批色譜填料(來自不同批次的顆?；w)以判斷一個分析方法的耐受性，可靠性和一致性。
來自三個不同批次的填料基體的三個不同批次的鍵合處理的ACQUITY UPLC柱對氯氨平有關物質的分析表現出zhuo越的重現性，保證了分析方法的長期重現性。
| 選擇性(a) | ||||
| 批號 | 雜質C | 雜質A | 氯氨平 | 雜質B |
| 119 | 1.03 | 1.07 | 1.07 | 1.59 |
| 120 | 1.03 | 1.07 | 1.07 | 1.58 |
| 124 | 1.02 | 1.07 | 1.07 | 1.58 |
ACQUITY UPLC方法驗證系統(tǒng)包
訂貨信息：
ACQUITY UPLC方法開發(fā)套裝[MDK: Method Development Kit]
| 套裝名稱 | 數量 | 固定相 | 顆粒大小 | 配置 | 部件編號 |
| 選擇性*大化大化UPLC方法開發(fā)套裝：寬泛的選擇性用于方法開發(fā)，包括在低pH和高pH下。是低離子強度添加劑條件時(例如甲酸)的*佳佳選擇 | |||||
| 選擇性*大化UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB | CSH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176002123 |
| 選擇性*大化UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB | CSH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176002124 |
| 選擇性*大化UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB | CSH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176002125 |
| 選擇性*大化UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB | CSH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176002126 |
| 高&低pH，寬選擇性的UPLC色譜柱套裝：通過開拓低和高流動相pH使分離選擇性寬 | |||||
| 高&低pH，寬選擇性的UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH C8, BEH Shield RP18, BEH苯基 | BEH 1.7 μm | 2.1 x 50 mm | 176001042 |
| 高&低pH，寬選擇性的UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH C8, BEH Shield RP18, BEH苯基 | BEH 1.7 μm | 2.1 x 100 mm | 176001043 |
| 高&低pH，寬選擇性的UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH C8, BEH Shield RP18, BEH苯基 | BEH 1.7 μm | 3.0 x 50 mm | 176001881 |
| 高&低pH，寬選擇性的UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH C8, BEH Shield RP18, BEH苯基 | BEH 1.7 μm | 3.0 x 100 mm | 176001882 |
| UPLC方法開發(fā)套裝：通過開拓低和高流動相pH(BEH色譜柱)將分離選擇性*大化大化和適用于極性化合物保留性(HSS T3) | |||||
| UPLC方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH 苯基, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176001603 |
| UPLC方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH 苯基, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176001604 |
| UPLC方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH 苯基, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176001883 |
| UPLC方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH 苯基, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176001884 |
| L1 UPLC色譜柱套裝：依從USP藥典中L1類別，但提供不同硅醇基活性和疏水性的C18色譜柱 | |||||
| L1 UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH Shield RP18, HSS C18, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176001605 |
| L1 UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH Shield RP18, HSS C18, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176001606 |
| L1 UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH Shield RP18, HSS C18, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176001885 |
| L1 UPLC色譜柱套裝 | 4件/包 | BEH C18, BEH Shield RP18, HSS C18, HSS T3 | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176001886 |
| 質譜UPLC色譜柱套裝：直鏈烷烴C18柱，具有不同的硅醇活性、峰形、選擇性和疏水性，且無MS流失問題 | |||||
| 質譜UPLC色譜柱套裝 | 4件/包 | BEH C18, HSS C18, HSS T3, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176001607 |
| 質譜UPLC色譜柱套裝 | 4件/包 | BEH C18, HSS C18, HSS T3, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176001608 |
| 質譜UPLC色譜柱套裝 | 4件/包 | BEH C18, HSS C18, HSS T3, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176001887 |
| 質譜UPLC色譜柱套裝 | 4件/包 | BEH C18, HSS C18, HSS T3, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176001888 |
| 低pH，寬選擇性UPLC色譜柱套裝：有各種不同的鍵合相和選擇性，用于開發(fā)低pH流動相條件下的反相方法 | |||||
| 低pH，寬選擇性UPLC色譜柱套裝 | 4件/包 | BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176001609 |
| 低pH，寬選擇性UPLC色譜柱套裝 | 4件/包 | BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176001610 |
| 低pH，寬選擇性UPLC色譜柱套裝 | 4件/包 | BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176001889 |
| 低pH，寬選擇性UPLC色譜柱套裝 | 4件/包 | BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176001890 |
| 選擇性*大化大化的RP 和 HILIC UPLC方法開發(fā)套裝：通過綜合HILIC和RP固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物 | |||||
| 選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, BEH Amide | CSH 1.7 μm; BEH 1.7 μm | 2.1 x 50 mm | 176002127 |
| 選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, BEH Amide | CSH 1.7 μm; BEH 1.7 μm | 2.1 x 100 mm | 176002128 |
| 選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, BEH Amide | CSH 1.7 μm; BEH 1.7 μm | 3.0 x 50 mm | 176002129 |
| 選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝 | 4件/包 | CSH C18, CSH苯己基, CSH氟苯基, BEH Amide | CSH 1.7 μm; BEH 1.7 μm | 3.0 x 100 mm | 176002130 |
| UPLC RP和HILIC方法開發(fā)套裝：通過綜合RP和HILIC固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物 | |||||
| UPLC RP和HILIC 方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 50 mm | 176001959 |
| UPLC RP和HILIC 方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 2.1 x 100 mm | 176001960 |
| UPLC RP和HILIC 方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 50 mm | 176001961 |
| UPLC RP和HILIC 方法開發(fā)套裝 | 4件/包 | BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB | BEH 1.7 μm; HSS 1.8 μm | 3.0 x 100 mm | 176001962 |
| UPLCHILIC方法開發(fā)套裝：在低pH(對堿性分析物)和高pH(對酸性分析物)下為極性和/或可離子化化合物輕松開發(fā)HILIC方法 | |||||
| UPLCHILIC方法開發(fā)套裝 | 4件/包 | BEH Amide, BEH HILIC | BEH 1.7 μm | 2.1 x 50 mm | 176001963 |
| UPLCHILIC方法開發(fā)套裝 | 4件/包 | BEH Amide, BEH HILIC | BEH 1.7 μm | 2.1 x 100 mm | 176001964 |
| UPLCHILIC方法開發(fā)套裝 | 4件/包 | BEH Amide, BEH HILIC | BEH 1.7 μm | 3.0 x 50 mm | 176001965 |
| UPLCHILIC方法開發(fā)套裝 | 4件/包 | BEH Amide, BEH HILIC | BEH 1.7 μm | 3.0 x 100 mm | 176001966 |
ACQUITY UPLC方法轉換套裝[MTK: Method Transfer Kit]*
| 套裝名稱 | UPLC Column 2.1 mm ID | HPLC Column 4.6 mm ID | 部件編號 |
| CSH C18 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186005529 |
| CSH Phenyl-Hexyl 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186005530 |
| CSH Fluoro-Phenyl 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186005531 |
| BEH C18 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186004958 |
| BEH Shield RP18 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186004959 |
| BEH HILIC 1.7 to 5 μm MTK | 50 mm, 1.7 μm | 150 mm, 5 μm | 186004960 |
| HSS C18 1.8 to 5 μm MTK | 50 mm, 1.8 μm | 150 mm, 5 μm | 186004961 |
| HSS T3 1.8 to 5 μm MTK | 50 mm, 1.8 μm | 150 mm, 5 μm | 186004962 |
| HSS C18 SB 1.8 to 5 μm MTK | 50 mm, 1.8 μm | 150 mm, 5 μm | 186004963 |
| HSS Cya.8 to 5 μm MTK | 50 mm, 1.8 μm | 150 mm, 5 μm | 186005979 |
| HSS PFP 1.8 to 5 μm MTK | 50 mm, 1.8 μm | 150 mm, 5 μm | 186006000 |
| CSH C18 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186005532 |
| CSH Phenyl-Hexyl 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186005533 |
| CSH Fluoro-Phenyl 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186005534 |
| BEH C18 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186004964 |
| BEH Shield RP18 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186004965 |
| BEH HILIC 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186004966 |
| BEH Amide 1.7 to 3.5 μm MTK | 50 mm, 1.7 μm | 100 mm, 3.5 μm | 186004967 |
| HSS C18 1.8 to 3.5 μm MTK | 50 mm, 1.8 μm | 100 mm, 3.5 μm | 186004968 |
| HSS T3 1.8 to 3.5 μm MTK | 50 mm, 1.8 μm | 100 mm, 3.5 μm | 186004969 |
| HSS C18 SB 1.8 to 3.5 μm MTK | 50 mm, 1.8 μm | 100 mm, 3.5 μm | 186004970 |
| HSS Cya.8 to 3.5 μm MTK | 50 mm, 1.8 μm | 100 mm, 3.5 μm | 186005980 |
| HSS PFP 1.8 to 3.5 μm MTK | 50 mm, 1.8 μm | 100 mm, 3.5 μm | 186006001 |
| CSH C18 1.7 to 3.5 μm High Rs MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186005535 |
| CSH Phenyl-Hexyl 1.7 to 3.5 μm高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186005536 |
| CSH Fluoro-Phenyl 1.7 to 3.5 μm高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186005537 |
| BEH C18 1.7 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004971 |
| BEH Shield RP18 1.7 to 3.5 μm高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004972 |
| BEH HILIC 1.7 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004973 |
| BEH Amide 1.7 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004974 |
| HSS C18 1.8 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004975 |
| HSS T3 1.8 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004976 |
| HSS C18 SB 1.8 to 3.5 μm 高分辨 MTK | 100 mm, 1.7 μm | 150 mm, 3.5 μm | 186004977 |
| HSS Cya.8 to 3.5 μm 高分辨 MTK | 100 mm, 1.8 μm | 150 mm, 3.5 μm | 186005981 |
| HSS PFP 1.8 to 3.5 μm 高分辨 MTK | 100 mm, 1.8 μm | 150 mm, 3.5 μm | 186006002 |
*每個套裝都含有一根UPLC色譜柱和一根HPLC色譜柱，可從ACQUITY UPLC在線社區(qū)
www.waters。。ｃｏｍ/myuplc下載ACQUITY UPLC Columns Calculator用于計算方法轉移。
ACQUITY UPLC方法驗證套裝[MVK:Method Validation Kit]**
| 固定相 | 粒徑 | 色譜柱長度 | 部件編號 2.1 mm ID | 部件編號 3.0 mm ID |
| CSH C18 | 1.7 μm | 50 mm | 186005571 | 186005573 |
| CSH C18 | 1.7 μm | 100 mm | 186005572 | 186005574 |
| CSH 苯己基 | 1.7 μm | 50 mm | 186005579 | 186005581 |
| CSH 苯己基 | 1.7 μm | 100 mm | 186005580 | 186005582 |
| CSH 氟苯基 | 1.7 μm | 50 mm | 186005575 | 186005577 |
| CSH 氟苯基 | 1.7 μm | 100 mm | 186005576 | 186005578 |
| BEH C18 | 1.7 μm | 50 mm | 186004044 | 186004691 |
| BEH C18 | 1.7 μm | 100 mm | 186004045 | 186004692 |
| BEH C8 | 1.7 μm | 50 mm | 186004046 | 186004693 |
| BEH C8 | 1.7 μm | 100 mm | 186004047 | 186004694 |
| BEH Shield RP18 | 1.7 μm | 50 mm | 186004048 | 186004695 |
| BEH Shield RP18 | 1.7 μm | 100 mm | 186004049 | 186004696 |
| BEH Phenyl | 1.7 μm | 50 mm | 186004050 | 186004697 |
| BEH Phenyl | 1.7 μm | 100 mm | 186004052 | 186004698 |
| BEH HILIC | 1.7 μm | 50 mm | 186004053 | 186004699 |
| BEH HILIC | 1.7 μm | 100 mm | 186004054 | 186004700 |
| BEH Amide | 1.7 μm | 50 mm | 186004807 | 186004809 |
| BEH Amide | 1.7 μm | 100 mm | 186004808 | 186004810 |
| BEH130 C18 | 1.7 μm | 100 mm | 186004896 | - |
| BEH300 C18 | 1.7 μm | 100 mm | 186004897 | - |
| BEH300 C4 | 1.7 μm | 100 mm | 186004899 | - |
| 寡核苷酸 C18 | 1.7 μm | 100 mm | 186004898 | - |
| Glycan BEH Amide | 1.7 μm | 100 mm | 186004907 | - |
| HSS T3 | 1.8 μm | 50 mm | 186004055 | 186004701 |
| HSS T3 | 1.8 μm | 100 mm | 186004056 | 186004702 |
| HSS C18 | 1.8 μm | 50 mm | 186004057 | 186004703 |
| HSS C18 | 1.8 μm | 100 mm | 186004058 | 186004704 |
| HSS C 18 SB | 1.8 μm | 50 mm | 186004137 | 186004705 |
| HSS C 18 SB | 1.8 μm | 100 mm | 186004138 | 186004709 |
| HSS PFP | 1.8 μm | 50 mm | 186005975 | - |
| HSS PFP | 1.8 μm | 100 mm | 186005976 | - |
| HSS PFP | 1.8 μm | 50 mm | 186005977 | - |
| HSS PFP | 1.8 μm | 100 mm | 186005978 | - |
| HSS 氰基 | 1.8 μm | 50 mm | 186005996 | 186005998 |
| HSS 氰基 | 1.8 μm | 100 mm | 186005997 | 186005999 |
**每個套裝包括來自3個不同批次填料的3根色譜柱。
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